Spiro[1,1a,6,6a-Tetrahydrocyclopropa[a]indene-1,1′-2′,3′-dihydro-1′H-indene]
✍ Scribed by Jovanovic, Jovan ;Elling, Wilhelm ;Schürmann, Markus ;Preut, Hans ;Spiteller, Michael
- Publisher
- International Union of Crystallography
- Year
- 2001
- Tongue
- English
- Weight
- 197 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 291 K Mean '(C±C) = 0.002 A Ê R factor = 0.046 wR factor = 0.140 Data-to-parameter ratio = 18.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal synchrotron study T = 100 K Mean '(C±C) = 0.004 A Ê R factor = 0.025 wR factor = 0.071 Data-to-parameter ratio = 8.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 16 H 13 ClO 2 , the tetrahydrobenzene ring adopts a boat conformation, and both cyclopropyl groups are orthogonal to the cyclobutane ring. The Cl atom shows positional disorder.
Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.003 A Ê R factor = 0.078 wR factor = 0.199 Data-to-parameter ratio = 15.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The solid-state conformation of the title compound, C 15 H 15 NO 4 S, has been established by X-ray crystallography. The orientation of the sulfonyl moiety is defined by the C-S-N-C torsion angle of À108.24 (16) . The angle between the naphthyl ring and the direction of the S-N bond is 71.24 (18) .