The dynamics of the liquid crystal director in "near magic angle" sample spinning has been investigated in mesophases with positive and negative diamagnetic susceptibility anisotropies and their mixtures with near-zero macroscopic diamagnetic anisotropy. To this end the deuteron quadrupolar splittin
✦ LIBER ✦
Spinning near the magic angle: a means of obtaining first-order dipolar NMR spectra of molecules dissolved in nematic liquid crystals
✍ Scribed by Courtieu, Jacques; Alderman, D. W.; Grant, David M.
- Book ID
- 115491850
- Publisher
- American Chemical Society
- Year
- 1981
- Tongue
- English
- Weight
- 279 KB
- Volume
- 103
- Category
- Article
- ISSN
- 0002-7863
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## Abstract It is demonstrated that in a case where neither the proton nor the natural‐abundance ^13^C‐satellite spectra of a partially oriented molecule carry enough structural information, one can determine the entire molecular geometry by the combined use of several liquid crystals as solvents.