Spin-locking spectral lineshapes of the central transition of half-integer quadrupole systems under magic-angle spinning
✍ Scribed by Shangwu Ding; Charles A. McDowell
- Publisher
- Elsevier Science
- Year
- 1995
- Tongue
- English
- Weight
- 569 KB
- Volume
- 355
- Category
- Article
- ISSN
- 0022-2860
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## Abstract Variable‐angle sample‐spinning (VASS) NMR was investigated for the case of limited rotation speed of the spinner. Side‐band intensities and line‐shapes for the central transition of half‐integer quadrupolar spin nuclei were calculated as a function of the parameter \documentclass{articl
## Abstract A simple procedure is presented for the determination of the asymmetry parameter of the electric field gradient, the quadrupole coupling constant, the second‐order quadrupolar shift and the isotropic chemical shift of quadrupolar nuclei with half‐integer spin directly from the experimen