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Spin-lattice relaxation of 13C in solid amino acids using the CP-MAS technique

✍ Scribed by A Naito; S Ganapathy; K Akasaka; C.A McDowell

Publisher
Elsevier Science
Year
1983
Weight
633 KB
Volume
54
Category
Article
ISSN
0022-2364

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13C CP/MAS NMR study of a phenyl group r
13C CP/MAS NMR study of a phenyl group rotation in the solid state using T1ρ, lineshape and 2D EXSY measurements
✍ Frank G. Riddell; Murray Bremner; John H. Strange πŸ“‚ Article πŸ“… 1994 πŸ› John Wiley and Sons 🌐 English βš– 316 KB

## Abstract A combination of solid‐state ^13^C CP/MAS NMR methods was used to study the rates of rotation of the phenyl group in 3,5‐dimethyl‐1‐phenylhex‐1‐yn‐3‐ol. The methods used were __T__~1ρ~ measurements, lineshape analysis and 2D exchange spectroscopy over the temperature range 219–284 K. Th