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Spin echo spectroscopic electron paramagnetic resonance imaging

โœ Scribed by Colin Mailer; Subramanian V. Sundramoorthy; Charles A. Pelizzari; Howard J. Halpern


Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
799 KB
Volume
55
Category
Article
ISSN
0740-3194

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โœฆ Synopsis


Abstract

The use of spin echoes to obtain spectroscopic EPR images (spectralโ€“spatial images) at 250 MHz is described. The advantages of spin echoesโ€”larger signals than the free induction decay, better phase characteristics for Fourier transformation, and decay shapes undistorted by instrumental dead timeโ€”are clearly shown. An advantage is gained from using a crossed loop resonator that isolates the 250โ€W pump power by greater than 50 dB from the observer arm preamplifiers. The echo decay rates can be used to determine the oxygen content in solutions containing 1 mM trityl concentrations. Twoโ€ and threeโ€dimensional images of oxygen concentration are presented. Magn Reson Med, 2006. ยฉ 2006 Wileyโ€Liss, Inc.


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