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Spectrophotometric determination of niobium in zirconium with 4-(2-pyridylazo)resorcinol

✍ Scribed by P. Pakalns; A.B. Ivanfy


Publisher
Elsevier Science
Year
1968
Tongue
English
Weight
508 KB
Volume
41
Category
Article
ISSN
0003-2670

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✦ Synopsis


iicigtrls. N.S. IV. (R rtstraliu) (Rcccivcd October xqth, xgG7) ELWELL AND WOODI

described the determination of 27% niobium in zirconium alloys, based on the formation of a yellow-coloured complex when niobium ions react with pyrogallol in an alkaline solution of ammonium oxalate; zirconium metal is dissolved by fusion with potassium hydrogen sulphate, for which finely divided samples are essential. WOOD

AND ADAMS~

Buff& solution, PIT 6.2. Dissolve 80 g of ammonium acetate in water, add 6.0


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Spectrophotometric determination of acid
✍ J. Ghasemi; A. Niazi; M. Kubista; A. Elbergali πŸ“‚ Article πŸ“… 2002 πŸ› Elsevier Science 🌐 English βš– 155 KB

The acidity constants of 4-(2-pyridylazo)resorcinol (PAR, Scheme 1) in binary mixtures of methanol-water at 25 β€’ C and an ionic strength of 0.1 M have been determined spectrophotometrically. DATa ANalysis (DATAN) program applied for determination of acidity constants. As percent of methanol increase