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Spectrophotometric and Nuclear Magnetic Resonance Study of Temperature- and Pressure-induced Changes in the Intimate Solvation of Neodymium (III) in N, N-Dimethylformamide and Trimethylphosphate

✍ Scribed by Dino L. Pisaniello; Peter J. Nichols; Yves Ducommun; André E. Merhach


Publisher
John Wiley and Sons
Year
1982
Tongue
German
Weight
162 KB
Volume
65
Category
Article
ISSN
0018-019X

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✦ Synopsis


Abstract

The temperature‐ and pressure‐dependent equilibria for the addition of an extra N, N‐dimethylforrnamide (DMF) or trimethylphosphate (TMP) ligand onto [Nd (DMF)~8~]^3+^‐ and [Nd(TMP)~6~]^3+^‐species respectively have been measured by visible spectrophotometry. Complementary NMR. studies on other lanthanide ions show a gradual shift in preference for the lower coordination number across the lanthanide series.