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Spectral properties of exo- and endo-tricyclo[3.2.1.02,4]octan-8-ones

✍ Scribed by Richard E. Pincock; John Haywood-Farmer

Publisher: Elsevier Science
Year: 1967
Tongue: French
Weight: 214 KB
Volume: 8
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)89598-8

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✦ Synopsis

The interaction of formally nonconjugated p-orbital systems has been observed in ultraviolet spectra &.g., changes in n + v* * and II + II transition energies and intensities for C=C-C-C=0 structures (2) ) as well as in increased rates of carbonium ion reactions (=.g., solvolysia of homoallylic structures C-C-C-C-X (3) ). The most outstanding example of the

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## Abstract Tricyclo[3.2.1.0^2,7^]octan‐3‐ol (**1**) and its 4‐isomer **7** were obtained by hydroboration of tricyclo[3.2.1.0^2,7^]oct‐3‐ene (**5**). The former alcohol **1** is quantitatively converted to the isomeric alcohol __exo__‐bicyclo[3.2.1]oct‐2‐en‐7‐ol (**3**) by treatment with aqueous a