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Spectral and luminescent properties of mixed-ligand complexes of palladium(II) and 7,8-benzoquinoline

✍ Scribed by M. V. Puzyk; V. S. Kotlyar; N. V. Antonov; Yu. A. Ivanov; M. A. Ivanov; K. P. Balashev

Book ID
110125429
Publisher
SP MAIK Nauka/Interperiodica
Year
2000
Tongue
English
Weight
46 KB
Volume
89
Category
Article
ISSN
0030-400X

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## Displacement of the chloride ligands from [Pd(q3all)Cl]2 (all = allyl, 2-methylallyl or 1,3-dimethylallyl) by treatment with AgNO, or AgC104 gives acetone-soluble species. These were not isolated but were reacted with 7,8-benzoquinoline (bquin) or 8-methylquinoline (8-Mequin) to give complexes of

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The complexes [(PhZdtc)Pd(R,mtc)ZPd(Phzdtc)] , Pd(Rzmtc)(R;dtc)(PPhJ) and Pd(az)(Rzmtc) have been prepared (az = azobenzene-2-C,N; R = methyl, R2 = pyrrolidyl, piperidyl and R ' = phenyl, ethyl, butyl). Infrared data reveal that in the solid state the [(Ph,dtc)Pd(R2mtc)ZPd(PhZdtc)] complexes are di