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Spectra and structure of organogermanes: 21—Infrared and Raman spectra, and vibrational assignment of (CH3)3GeNNN and Normal coordinate calculations of (CH3)3GeNNN, (CH3)3GeNCO and (CH3)3GeNCS

✍ Scribed by J. R. Durig; M. R. Jalilian; J. F. Sullivan; J. B. Turner

Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
919 KB
Volume
11
Category
Article
ISSN
0377-0486

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## Abstract Raman spectra of 1,3‐disilabutane (SiH~3~CH~2~SiH~2~CH~3~) as a liquid were recorded at 293 K and as a solid at 78 K. In the Raman cryostat at 78 K an amorphous phase was first formed, giving a spectrum similar to that of the liquid. After annealing to 120 K, the sample crystallized and