Specific Isotope Enrichment of Methyl Methacrylate

✍ Scribed by Thekla M. Werkhoven; Reinier van Nispen; Johan Lugtenburg

• Publisher: John Wiley and Sons
• Year: 1999
• Tongue: English
• Weight: 236 KB
• Volume: 1999
• Category: Article
• ISSN: 1434-193X
• DOI: 10.1002/(sici)1099-0690(199911)1999:11<2909::aid-ejoc2909>3.0.co;2-5

✦ Synopsis

Keywords: Methyl methacrylate / 13 C label / Mass spectrometry / 1 H NMR / 13 C NMR A synthetic scheme has been developed to prepare methyl scheme methyl (1-13 C)-and methyl (2-13 C)methacrylate (1a and 1b) have been prepared with high label incorporation methacrylate specifically 13 C-labelled at all different positions and in any combination of positions, from simple, (99%). commercially available starting materials. According to this poly(styrene-co-maleic anhydride). Also crosslinking of [a