𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Spalling failure of a thermal barrier coating associated with aluminum depletion in the bond-coat

✍ Scribed by E.A.G Shillington; D.R Clarke


Publisher
Elsevier Science
Year
1999
Tongue
English
Weight
800 KB
Volume
47
Category
Article
ISSN
1359-6454

No coin nor oath required. For personal study only.

✦ Synopsis


AbstractÐA plasma-sprayed thermal barrier coating is observed to spall after oxidation at 11218C from a CoNiCrAlY bond-coated superalloy at the interface between the thermally grown oxide (TGO) and the zirconia thermal barrier coating (TBC). Phase characterization by photostimulated luminescence and X-ray diraction, as well as microstructural characterization by scanning electron microscopy, indicates that the spalling is associated with the conversion of the initially formed a-alumina thermally grown oxide to achromia and a goxi grel spinel. It is proposed that the phase conversion occurs after the alumina TGO has cracked on thermal cycling and the underlying bond-coat alloy is depleted of aluminum with concurrent enrichment of the oxide by Cr, Co and Ni. The observations suggest that monitoring the luminescence intensity as a function of oxidation time might form the basis of a nondestructive tool for detecting the onset of failure based on the disappearance of a-alumina.