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Solvothermal Synthesis, Crystal Structure, and Properties of the New Oxothiomolybdate Ni(dien)2[Mo2O2S6]

✍ Scribed by Jan Ellermeier; Wolfgang Bensch

Book ID: 106214957
Publisher: Springer Vienna
Year: 2001
Tongue: English
Weight: 162 KB
Volume: 132
Category: Article
ISSN: 0026-9247
DOI: 10.1007/s007060170094

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## Abstract Two 2D Anderson polyoxomolybdate‐based compounds, [{Ni(H~2~O)~4~}~2~{Ni(OH)~6~Mo~6~O~18~}]·4H~2~O (1) and [Ni(H~2~O)~6~][Ag~2~{Ni(OH)~6~Mo~6~O~18~}]·8H~2~O (2), were synthesized and characterized by elemental analysis, IR spectroscopy, SEM, and single‐crystal XRD. Their thermal behavior