Intramolecular Base Stabilization of Sil
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Dr. Claude Chuit; Prof. Dr. Robert J. P. Corriu; Ahmad Mehdi; Dr. Catherine Reyé
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Article
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1993
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John Wiley and Sons
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English
⚖ 332 KB
👁 1 views
To a hydrogenation vessel. filled with Raney Cobalt catalyst (Cr promoted. Grace 2724. pretreated with hydroxide. YO0 g) and wafer (22.5 L) was iidded DAB-r/mdr-(CN), (450 g) dissolved in methanol. Subsequentl! the mixture was hydrogenated at 40 atm hydrogen pressure at 70 C for 1 h. The cooled reac