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Solving Larger Molecular Crystal Structures from Powder Diffraction Data by Exploiting Anisotropic Thermal Expansion

✍ Scribed by Michela Brunelli; Jonathan P. Wright; Gavin B. M. Vaughan; Asiloe J. Mora; Andrew N. Fitch

Book ID: 101531308
Publisher: John Wiley and Sons
Year: 2003
Tongue: English
Weight: 129 KB
Volume: 115
Category: Article
ISSN: 0044-8249
DOI: 10.1002/ange.200250607

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The ordered, low-temperature crystal structure of the pure enantiomer of camphor (C 10 H 16 O) has been solved from highresolution powder synchrotron X-ray di4raction data. The structure is orthorhombic, space group P2 1 2 1 2 1 , Z ‫؍‬ 8, with a ‫؍‬ 8.9277(2) A s , b ‫؍‬ 27.0359(5) A s , and c ‫؍‬