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Solventless injecction for packed column supercritical fluid chromatography

✍ Scribed by Dean, T. A. ;Poole, C. F.

Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
604 KB
Volume
12
Category
Article
ISSN
0935-6304

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✦ Synopsis

The adverse effects of injection solvent strength on microbore packed column SFC band broadening are demonstrated and a solventless injection system that eliminates these effects is introduced. The injection system removes solvent in a GC-like manner using a retention gap and an on-column capillary GC syringe. The analyte is delivered to the analytical column in a solvent-free plug of supercritical fluid mobile phase.

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