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Solvent Trapping during Large Volume Injection with an Early Vapor Exit, Part 2: Chromatographic Results and Conclusions

✍ Scribed by Grolimund, Beat ;Boselli, Emanuele ;Grob, Konrad ;Amadò, Renato ;Lercker, Giovanni


Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
69 KB
Volume
21
Category
Article
ISSN
0935-6304

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Solvent Trapping during Large Volume Inj
✍ Boselli, Emanuele ;Grob, Konrad ;Lercker, Giovanni 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 116 KB

When 0.53 mm i.d. uncoated precolumns connected to a solvent vapor exit are used for sample introduction with partially concurrent solvent evaporation, substantial losses of volatile solutes are often observed. They were found to be the consequence of solute accumulation at the front end of the floo