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Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis

✍ Scribed by Fabbiani, Francesca P. A.; Byrne, Lindsay T.; McKinnon, Joshua J.; Spackman, Mark A.


Book ID
118057314
Publisher
Royal Society of Chemistry
Year
2007
Tongue
English
Weight
412 KB
Volume
9
Category
Article
ISSN
1466-8033

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A simple molecule with a complex crystal
✍ Klaus Eichele; Christiane Nachtigal; Susanne Jung; Hermann A. Mayer; Ekkehard Li 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 174 KB

## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should