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Solvent-Free Synthesis of 2-Furyl-5-aryloxyacetylamido-1,3,4-thiadiazoles Under Microwave Irradiation

✍ Scribed by Wang, Xicun; Li, Zheng; Quan, Zhengjun; Lu, Xinsheng; Gou, Ruhu


Book ID
120980343
Publisher
Taylor and Francis Group
Year
2003
Tongue
English
Weight
167 KB
Volume
33
Category
Article
ISSN
0039-7911

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## Abstract The one pot, three‐components condensation of aromatic aldehydes, hydrazine and sulfur in ethanol under microwave irradiation provided symmetrically 3,5‐disubstituted 1,3,4‐thiadiazoles in high yields and good purity. This reaction must be conducted under pressure of hydrogen sulfide pr