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Solvent free synthesis of 1,5-benzodiazepine derivatives over the heterogeneous silver salt of silicotungstic acid under ambient conditions

✍ Scribed by Jadhav, Arvind H.; Kim, Hern

Book ID: 120544353
Publisher: The Royal Society of Chemistry
Year: 2013
Tongue: English
Weight: 765 KB
Volume: 3
Category: Article
ISSN: 2046-2069
DOI: 10.1039/C3RA22663H

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## Abstract It is described that sulfamic acid can be utilized as an effective and green catalyst for the synthesis of 1,5‐benzodiazepines in high yields from the solvent‐free condensation of o‐phenylenediamine (**1**) and ketones (**2**). © 2007 Wiley Periodicals, Inc. Heteroatom Chem 18:354–358,