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Solvent-free synthesis of 1-(p-toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-one from Dess–Martin periodinane and its synthetic utility for α-tosyloxylation of ketones

✍ Scribed by Nandkishor N. Karade; Girdharilal B. Tiwari; Sandeep V. Shinde; Sumeet V. Gampawar; Jeevan M. Kondre

Book ID: 104095262
Publisher: Elsevier Science
Year: 2008
Tongue: French
Weight: 106 KB
Volume: 49
Category: Article
ISSN: 0040-4039
DOI: 10.1016/j.tetlet.2008.03.119

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✍ Nandkishor N. Karade; Girdharilal B. Tiwari; Sandeep V. Shinde; Sumeet V. Gampaw 📂 Article 📅 2008 🏛 John Wiley and Sons ⚖ 32 KB 👁 1 views

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✍ Nandkishor N. Karade; Girdharilal B. Tiwari; Sandeep V. Shinde; Sumeet V. Gampaw 📂 Article 📅 2008 🏛 Elsevier Science 🌐 French ⚖ 115 KB

The authors regret that the reaction of Dess-Martin periodinane with p-toluenesulfonic acid monohydrate using a grinding technique does not lead to the formation of 1-(p-toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-one 8 as reported in the above Letter. 1-(p-Toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-on