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Solvent-free microwave-assisted Beckmann rearrangement of benzaldehyde and 2-hydroxyacetophenone oximes

✍ Scribed by André Loupy; Serge Régnier

Book ID
104261942
Publisher
Elsevier Science
Year
1999
Tongue
French
Weight
264 KB
Volume
40
Category
Article
ISSN
0040-4039

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✦ Synopsis

Beckmann rearrangements of benzaldehyde and 2-hydroxyacetophenone were largely improved by performing solvent-free reactions in the presence of one equivalent of anhydrous zinc chloride. When compared to conventional heating under the same conditions, yields are significantly enhanced under microwave activation.

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