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Solvent effect on epoxidation of allyl chloride with hydrogen peroxide on titanium-containing silicalite

✍ Scribed by S. M. Danov; A. V. Sulimov; A. V. Sulimova

Book ID
111462590
Publisher
SP MAIK Nauka/Interperiodica
Year
2008
Tongue
English
Weight
181 KB
Volume
81
Category
Article
ISSN
1070-4272

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## Abstract Titanium silicalite‐1 (TS‐1) films were prepared on SiO~2~ pellet supports via an __in situ__ hydrothermal synthesis method and were characterized by X‐ray diffraction (XRD), Fourier transform infrared spectroscopy (FT‐IR), scanning electron microscopy (SEM) and ^29^Si magic angle spinn

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## Abstract The influence of the technological parameters on the course of the epoxidation of allyl alcohol with 30% H~2~O~2~ in the presence of titanium silicalite TS‐2 catalyst and methanol as a solvent was studied. The process was performed in an autoclave at the autogenic pressure. The influenc