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Solid State NMR, X-Ray Diffraction, and Infrared Characterization of Local Structure in Heat-Treated Oxyhydroxyapatite Microcrystals: An Analog of the Thermal Decomposition of Hydroxyapatite during Plasma-Spray Procedure

✍ Scribed by P. Hartmann; C. Jäger; St. Barth; J. Vogel; K. Meyer


Publisher
Elsevier Science
Year
2001
Tongue
English
Weight
471 KB
Volume
160
Category
Article
ISSN
0022-4596

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✦ Synopsis


The structure of plasma-sprayed hydroxyapatites possesses a variety of partially dehydrated hydroxyapatite structures. Nuclear magnetic resonance, IR spectroscopy, and X-ray di4raction have been used to analyze the structure of partially dehydrated hydroxyapatites. The oxyhydroxyapatites are prepared from crystalline hydroxyapatite by thermal treatment in air. The obtained results enable an advanced phase analysis of plasmasprayed hydroxyapatite layers.