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Solid-State NMR Spectroscopy under Periodic Modulation by Fast Magic-Angle Sample Spinning and Pulses: A Review

✍ Scribed by S. Hafner; D.E. Demco

Publisher: Elsevier Science
Year: 2002
Tongue: English
Weight: 431 KB
Volume: 22
Category: Article
ISSN: 0926-2040
DOI: 10.1006/snmr.2002.0088

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✦ Synopsis

Fast magic-angle spinning (MAS) holds promise for new approaches to pulsed high-resolution NMR in solids where homogeneous interactions dominate. Prerequisite for developing new pulse methods is the understanding of signal encoding by spin interactions under MAS conditions and of interferences between MAS and pulses. This review discusses corresponding strategies and techniques in a coherent way with particular concentration on homonuclear decoupling techniques for line-narrowing in solids.

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