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Solid State and Gas Phase NMR Studies of Immobilized Catalysts and Catalytic Active Nanoparticles

โœ Scribed by Anna Adamczyk; Yeping Xu; Bernadeta Walaszek; Frank Roelofs; Tal Pery; Karin Pelzer; Karine Philippot; Bruno Chaudret; Hans-Heinrich Limbach; Hergen Breitzke; Gerd Buntkowsky


Publisher
Springer
Year
2008
Tongue
English
Weight
527 KB
Volume
48
Category
Article
ISSN
1022-5528

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The gas-phase basicities of 3,4,5-tri-tert-butylpyrazole (I) and 1,3,4,5-tetra-tert-butyl-pyrazole (11) were measured by Fourier transform ion cyclotron resonance spectrometry. The x-ray molecular structures of 1-HCI (a monohydrate) and I1 were determined. A clear lack of planarity is present in the