Solid-state 1H-static, 1H-MAS, and 1H→19F/19F→1H CP/MAS NMR study of poly(vinyl fluoride)
✍ Scribed by Shinji Ando; Robin K. Harris; Peter Holstein; Stefan A. Reinsberg; Kazuo Yamauchi
- Book ID
- 108366441
- Publisher
- Elsevier Science
- Year
- 2001
- Tongue
- English
- Weight
- 379 KB
- Volume
- 42
- Category
- Article
- ISSN
- 0032-3861
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Fluorine-19M1HN nuclear magnetic resonance (NMR) at 188.29 MHz, including 1H ] 19FM1HN crosspolarization (CP) with high-speed magic-angle spinning (MAS), was used to study some Ñuoropolymers of the Viton type. The systems examined were (a) copolymers of vinylidene Ñuoride and hexaÑuoropropene and (b
## Abstract The changes in the conformation and molecular mobility accompanied by a phase transition in the crystalline domain were analyzed for ethylene (E) and tetrafluoroethylene (TFE) copolymer, ETFE, using variable‐temperature (VT) solid‐state ^19^F magic angle spinning (MAS) and ^1^H → ^19^F