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Solid-phase synthesis of α-hydroxy phosphonates and hydroxystatine amides. Transition-state isosteres derived from resin-bound amino acid aldehydes

✍ Scribed by Roland E Dolle; Timothy F Herpin; Yvonne Class Shimshock


Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
125 KB
Volume
42
Category
Article
ISSN
0040-4039

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✦ Synopsis


Resin-bound N-acylated amino acid aldehydes iv were converted in a single step to a-hydroxy phosphonates vii (Pudovik reaction) and in six-steps to hydroxystatine amides viii, demonstrating the utility of intermediates iv for constructing multiple aspartic acid transition-state isosteres.