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Solid phase stereochemical dynamics of 18-crown-6 ether and its KNCS complex as studied by low temperature carbon-13 nuclear magnetic resonance

✍ Scribed by G.W. Buchanan; R.A. Kirby; J.A. Ripmeester; C.I. Ratcliffe


Publisher
Elsevier Science
Year
1987
Tongue
French
Weight
202 KB
Volume
28
Category
Article
ISSN
0040-4039

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✦ Synopsis


We r port resolution of individual carbon environments of 18-crown-6 ether and its KNCS complex using I5 C CPMAS nuclear magnetic resonance spectroscopy at low temperature.

The importance of torsional angle effects in determining chemical shifts in these solids is discussed.