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Sodium borohydride reduction of steroidal ketones with and without irradiation

✍ Scribed by Waters, James A.; Witkop, Bernhard.

Book ID
121447144
Publisher
American Chemical Society
Year
1968
Tongue
English
Weight
791 KB
Volume
90
Category
Article
ISSN
0002-7863

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## Abstract The rates for the reduction of ketones with sodium borohydride are interpreted in terms of two parameters, both derived from force‐field calculations; __i.e.__ the strain difference between alcohol and ketone (Ξ” strain) and the steric hindrance towards approach of the hydride R. Models

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## Abstract Aldehydes, ketones and imines were readily reduced by sodium borohydride, with the participation of a small amount of water, in good to excellent yields using PEG400 as catalyst in the absence of organic solvents. Copyright Β© 2005 Society of Chemical Industry