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Site of dopamine D1 receptor binding to GS protein mapped with synthetic peptides

✍ Scribed by Bernd König; Michael Grätzel

Book ID: 116106185
Publisher: Elsevier Science
Year: 1994
Tongue: English
Weight: 588 KB
Volume: 1223
Category: Article
ISSN: 0167-4889
DOI: 10.1016/0167-4889(94)90235-6

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Scheme 2. Synthesis of 2 a-c, e. Reagents and conditions: a) BF 3 •Et 2 O, Et 3 SiH, CH 2 Cl 2 , 08C, 1 h; b) BF 3 •Et 2 O, allylTMS, CH 2 Cl 2 , 258C, 2 h; c) CyMgCl or AdMgBr, 0 8C, 1 h; d) Mitsunobu conditions, 25 8C, 2 h; e) H 2 , Pd/C, EtOH, 1 atm, 25 8C, 24 h. Scheme 3. Attempted synthesis of