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Single-Crystal Structure Determination of Na4P2S6·6H2O

✍ Scribed by T. Fincher; G. LeBret; D.A. Cleary

Publisher
Elsevier Science
Year
1998
Tongue
English
Weight
454 KB
Volume
141
Category
Article
ISSN
0022-4596

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✦ Synopsis

The cell volume was calculated to be 3374.12(9) A s 3 , and the density was calculated to be 1.565 Mg/m 3 . The single crystal structure was also solved at ؊60°C. The low temperature crystal data were a ‫؍‬ 25.3961(3) A s , b ‫؍‬ 7.06480(10) A s , and c ‫؍‬ 20.22160(10) A s , ‫؍‬ 113.431(1)°, Z ‫؍‬ 8. The ؊60°C-cell volume was calculated to be 3328.95(6) A s 3 , and the density was calculated to be 1.586 Mg/m 3 .

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Growth and Characterization of Na2CaGe6O
Growth and Characterization of Na2CaGe6O14 Single Crystals
✍ Hiroaki Takeda; Reinhard Uecker; Makoto Kumatoriya; Kiyoshi Shimamura; Peter Rei 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 388 KB

## Abstract Transparent, crack‐free Na~2~CaGe~6~O~14~ (NCG) single crystals were successfully grown using the Czcchralski technique. The largest crystal had 30 mm in total length and 18 mm in maximal diameter. Best crystal quality was achieved under low temperature gradient arrangement. The crystal