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Simultaneous determination of non-volatile, semi-volatile, and volatile organic acids in tobacco by SIM–Scan mode GC–MS

✍ Scribed by Baoxing Wang; Shihua Yang; Guohui Chen; Yi Wu; Ying Hou; Guowang Xu

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
431 KB
Volume
31
Category
Article
ISSN
1615-9306

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✦ Synopsis

Abstract

A method for simultaneous determination of seven nonvolatile organic acids (NVOAs), five semivolatile organic acids (SVOAs), and twelve volatile organic acids (VOAs) in tobacco by synchronous SIM (Selected Ion Monitoring)‐scan mode GC–MS was developed. The collection of NVOAs and SVOAs data was performed in full‐scan mode, and that of VOAs data was carried out with SIM. Recoveries of NVOAs and SVOAs varied from 90.0 to 103.0%, and RSDs were less than 4.0%; recoveries of VOAs ranged from 89.5 to 99.3%, and their RSDs were less than 3.0%. Twelve tobacco samples were analyzed by the described method, and the results show that the method is applicable for the simultaneous determination of VOAs, NVOAs, and SVOAs in tobacco.

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