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Simplified sample preparation procedure for measuring isotope-enriched methylmercury by gas chromatography and inductively coupled plasma mass spectrometry

✍ Scribed by Mary-Luyza Avramescu; Joy Zhu; Emmanuel Yumvihoze; Holger Hintelmann; Danielle Fortin; David R.S. Lean


Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
138 KB
Volume
29
Category
Article
ISSN
0730-7268

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A novel interface design for coupling gas chromatography and inductively coupled plasma mass spectrometry (GC/ICP-MS) was used to perform mercury speciation in biological tissues. Three derivatization approaches were optimized and compared for this purpose: anhydrous butylation using a Grignard reag