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Simple Preparation of O-Substituted Hydroxylamines from Alcohols.

โœ Scribed by Sebastien Albrecht; Albert Defoin; Celine Tarnus

Book ID
101994562
Publisher
John Wiley and Sons
Year
2006
Weight
16 KB
Volume
37
Category
Article
ISSN
0931-7597

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โœฆ Synopsis

Abstract

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๐Ÿ“œ SIMILAR VOLUMES

Asymmetric reduction of ketoxime ethers
Asymmetric reduction of ketoxime ethers to optically active O-substituted hydroxylamines with reagents prepared from borane and chiral amino alcohols
โœ John T. Dougherty; Joseph R. Flisak; Jerome Hayes; Ivan Lantos; Li Liu; Lynn Tuc ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 183 KB

The asymmetric reduction of ketoxime ethers to yield enantiomerically enriched chiral hydroxylamines with reagents prepared from borane and norephedrine has been investigated. Very high enantioselectivity (ca. 99% ee) was obtained in the reduction of ketoxime O-(o-nitrobenzyl) ether to O-(o-nitroben