โ Scribed by Michael T Mai; Anthony Ribeiro; Oleg Jardetzky
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
Use of the deuterium NMR spectrum of a deuteriated solute dissolved in the nematic phase of a liquid crystal is suggested for setting the magic angle in solid state NMR. The use of the method as a convenient and accurate means of setting the angle is demonstrated.
## Abstract The mechanical and electronic design of a โmagic angleโ NMR probe is described. This probe can be incorporated in a conventional small gap ^13^C FT spectrometer, without any hardware or software change, to obtain high resolution ^13^C NMR spectra on organic solids. A simple way of tunin
## Abstract A simple procedure is presented for the determination of the asymmetry parameter of the electric field gradient, the quadrupole coupling constant, the secondโorder quadrupolar shift and the isotropic chemical shift of quadrupolar nuclei with halfโinteger spin directly from the experimen