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Simple and rapid GLC method for the determination of orphenadrine in human plasma

โœ Scribed by Manuela Contin; Roberto Riva; Fiorenzo Albani; Agostino Baruzzi

Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
224 KB
Volume
2
Category
Article
ISSN
0269-3879

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โœฆ Synopsis

A rapid and specific method has been developed for the determination of orphenadrine concentration in plasma. It involves a one-step sample preparation using n-hexane/isopropyl alcohol (98 : 2) extraction, and analysis by gas chromatography on a wide bore capillary column using nitrogen/phosphorus detection. This procedure considerably simplifies previously reported assays and is specific and sensitive enough for the determination of orphenadrine in plasma of patients on chronic therapy.

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However, there were significant correlations between the enthalpy involved and each of VAG maximum viscosity, breakdown, viscosity at 50 ยฐC and set back (r = 0.53, P < 0.05; r = 0.49, P < 0.05; r = 0.62, P < 0.05; r = 0.65, P < 0.01, respectively). For RVA data, correlations were found only between