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Silyl-Subsituted Sulfur Amides and Imides

โœ Scribed by Prof. Dr. U. Wannagat; Dipl.-Chem. H. Kuckertz

Publisher
John Wiley and Sons
Year
1962
Tongue
English
Weight
127 KB
Volume
1
Category
Article
ISSN
0044-8249

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โœฆ Synopsis

The infrared spectrum supports the carbodiimide structure, since the symmetrical NCN-and the asymmetrical SiNSi vibrations, which should occur for the structural isomer bis(trimethylsilyl)cyanarnide(R3Si~)~-C~N,are not present.

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On irradiation in the presence of Fe(CO),, the allenic amides and imides showed a similar course of complexation to that of esters and lactones, respectively, e.g. the amides of type 10 led to diiron complexes of type 11 (Scheme 3 ) , whereas the imide 12 yielded a mixture of a dinuclear and two mon