Silicon carbide hollow nanospheres, nanowires and coaxial nanowires
β Scribed by Guozhen Shen; Di Chen; Kaibin Tang; Yitai Qian; Shuyuan Zhang
- Publisher
- Elsevier Science
- Year
- 2003
- Tongue
- English
- Weight
- 298 KB
- Volume
- 375
- Category
- Article
- ISSN
- 0009-2614
No coin nor oath required. For personal study only.
β¦ Synopsis
The synthesis and characterization of hollow nanospheres, nanowires and coaxial nanowires of cubic phase silicon carbide (b-SiC) were reported. The reaction between SiCl 4 (or Si powders), C 6 Cl 6 and sodium was used to prepare SiC nanostructures at different temperature. The samples were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), electron diffraction (ED), high-resolution transmission electron microscopy (HRTEM), Raman, photoluminescence (PL) and X-ray photoelectron spectroscopy (XPS) procedures. Studies found that temperature and reagents were key factors for the samplesΓ morphologies.
π SIMILAR VOLUMES
Organic amines (decylamine, dodecylamine, octodecylamine) and titanium iso-propoxide (Ti( i OPr) 4 ) were purchased from Aldrich, and used without further treatment. Doubly distilled water and absolute ethanol were used as solvents. Synthesis: For the synthesis of mesoporous TiO 2 , 0.01 mol Ti( i