Sign determination of dipolar couplings in field-oriented bicelles by variable angle sample spinning (VASS)

Measurement of Interproton, Nuclear Spin

Measurement of Interproton, Nuclear Spin Dipolar Couplings in Liquid Crystalline Samples by Combining Variable Angle Sample Spinning, Isotope Dilution, and Deuterium Decoupling

✍ E. Ciampi; G. De Luca; J.W. Emsley 📂 Article 📅 1997 🏛 Elsevier Science 🌐 English ⚖ 138 KB

The proton NMR spectra of liquid crystalline samples can be but it has not been used to study a mesogenic molecule since simplified by selective, partial deuteration followed by deuterium these are not easily fully deuterated catalytically (5). The decoupling. This leaves strong peaks from the proto