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SFE of PAHs from soils with a high carbon content and analyte collectionvia combined liquid/solid trapping

✍ Scribed by Meyer, Anja ;Kleiböhmer, Wolfgang ;Cammann, Karl


Book ID
102352600
Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
384 KB
Volume
16
Category
Article
ISSN
0935-6304

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✦ Synopsis


Abstract

Polynuclear aromatic hydrocarbons (PAHs) are recovered from a soil with a high carbon content (ca. 50%) with supercritical fluid extraction (SFE) as well as with conventional Soxhlet extraction. The influence of temperature and modifier volume on SFE efficiency and the effect of a combined liquid/solid trap for analyte collection are investigated in this study. Such traps, which make analyte collection and clean‐up possible in one step, are compared with conventional analyte collection in pure organic solvents. A comparison between reproducibility and efficiency of SFE and Soxhlet extraction is presented.