Sequential hydrolysis of proline-containing peptides with immobilized aminopeptidases
β Scribed by Gideon Fleminger; Arieh Yaron
- Book ID
- 113264441
- Publisher
- Elsevier Science
- Year
- 1983
- Tongue
- English
- Weight
- 761 KB
- Volume
- 743
- Category
- Article
- ISSN
- 0167-4838
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π SIMILAR VOLUMES
A micromethod for nondestructive amino acid analysis was developed. Peptides were digested with amino-peptidase M followed by prolidase. The whole procedure was performed in a microvial for the autosampler of the analyzer. The resulting method has a working range from 10 to 600 pmol, at least, of sa
The N-acyi hydroqmerhylpyrrole amino acid analogues S-7 and 9 were synthesized via a mild DMAP caralysed acylalion of pyrrole-2-carboxaldehyde with an acid chloridefollowed byformyl group reduciion with Zn(BHq)2. The N-acyl subs&red hydroxy~e%ylpyrroies are aclivaied on hydrolysis to give an electro