𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Sensitivity-optimized experiment for the measurement of residual dipolar couplings between amide protons

✍ Scribed by Paul Schanda; Ewen Lescop; Mirjam Falge; Rémy Sounier; Jérôme Boisbouvier; Bernhard Brutscher

Book ID
106401456
Publisher
Springer Netherlands
Year
2007
Tongue
English
Weight
403 KB
Volume
38
Category
Article
ISSN
0925-2738

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Sensitivity-enhanced Experiments for the
Sensitivity-enhanced Experiments for the Measurement of J and Dipolar Coupling Constants
✍ Dong-Hai Lin; Xin-Li Liao 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 393 KB

## Abstract A sensitivity‐enhanced IPAP NMR experiment was described in this paper, which separates the ^1^H‐^15^N doublets into two different spectra to alleviate the problem of resonance overlaps and achieve the accurate measurement of __J__ and residual dipolar coupling constants in proteins. Th

J-modulated 1D directed COSY for precise
J-modulated 1D directed COSY for precise measurement of proton–proton residual dipolar coupling constants of oligosaccharides
✍ Tran N. Pham; Tibor Liptaj; Paul N. Barlow; Dušan Uhrín 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 107 KB

## Abstract A simple selective 1D experiment for the accurate and precise determination of residual proton–proton dipolar coupling constants of oligosaccharides is proposed. The technique is based on the concept of __J__‐modulated spectroscopy and provides coupling constants by fitting the peak int