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Semiconducting properties of the anodic Pb(ii) oxide film in alkaline solution

✍ Scribed by Xia Shen-Jiang; Zhou Wei-Fang

Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
430 KB
Volume
40
Category
Article
ISSN
0013-4686

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Effects of Samarium on the Properties of
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## Abstract The effects of samarium on the properties of the anodic Pb(II) oxides films formed on lead at 0.9 V (vs. Hg/Hg~2~SO~4~) in 4.5 mol/L H~2~SO~4~ solution were studied using linear sweep voltammetry (LSV), electrochemical impedance spectroscopy (EIS) and scanning electron micrographs (SEM)

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The reduction process of the anodic Pb(ii) oxide film on lead + bismuth alloy in sulfuric acid solution
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The anodic film studied was formed on Pb + 9at.%Bi at 0.9V (vs. Hg/Hg,S03 in 4.5 M H, SO, solution (25Β°C). The change of the phase composition of the anodic film during reduction at -0.91 V (vs. Hg/Hg,SO,) (slightly more positive than that of the reduction potential of PbSO,) was determined by X-ray