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Semi-Automated fluorometric assay for urinary total and b n-acetyl-β-d-glucosaminidase: Analytical investigation

✍ Scribed by William Kristz; Ghassan Joseph Samaan; Corinne Leberre; Jean-François Demelier; Daniel Biou


Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
188 KB
Volume
5
Category
Article
ISSN
0887-8013

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✦ Synopsis


Total N-acetyl-p-D-glucosaminidase (NAG) and NAG-B isoenzyme determination are determined in order to investigate renal tubular function. Here, we propose a semiautomated adaptation of Sandman's manual method for the Monarch centrifugal analyzer. Fluorescence of the released 4-methylumbelliferone is automatically read and results are directly expressed in nanokatalA. Mean (1 SD) values expressed in nanokatal/millirnole creatinine in urine from healthy female (n = 30) and male (n = 30) subjects were 8.2 (4.0) and 7.8 (2.9) for total NAG and 1.9 (1.4) and 1.5 (0.7) for the NAG-B isoenzyme activity. The assay of six patients with various renal disorders shows definite increase in total NAG and NAG-B isoenzyme activities.