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Selenocyanato Derivatives of Hydro-closo-borates: Syntheses and Crystal Structures of (PPh4)2[SeCN)BnHn–1] (n = 6, 10, 12)

✍ Scribed by Nachtigal, Christiane ;Steuer, Boris ;Preetz, Wilhelm

Publisher
Wiley (John Wiley & Sons)
Year
1996
Tongue
English
Weight
366 KB
Volume
129
Category
Article
ISSN
0009-2940

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Syntheses and Crystal Structures of the closo-Borates M 2 [B 7 H 7 ] and M[B 7 H 8 ] (M: PPh4, PNP, and N(n-Bu4)): The Missing Crystal Structure in the Series [BnHn] 2- (n: 6-12). -The first convenient synthesis of the seven-vertex closo-[B7H7] 2-anion via O2-oxidation of [B9H9] 2-is reported. Proto