Selective Sample Handling and Detection in High-Performance Liquid Chromatography

✍ Scribed by K. Zech and R.W. Frei (Eds.)

• Publisher: Elsevier, Academic Press
• Year: 1989
• Tongue: English
• Leaves: 407
• Series: Journal of Chromatography Library 39, Part B
• Category: Library

✦ Synopsis

This is the second of a two-volume project which treats the handling, separation and detection of complex samples as an integrated, interconnected process. On the basis of this philosophy the editors have selected those contributions which demonstrate that optimal sample preparation leads to a simplification of detection or reduced demands on the separation process. Throughout the book emphasis is on chemical principles with minimum discussion of the equipment required - an approach which reflects the editors' view that the limiting factor in the analysis of complex samples is an incomplete knowledge of the underlying chemistry rather than the hardware available. This lack of knowledge becomes more evident as the demands for lower detection limits grow, as solving complex matrix problems requires a greater understanding of the chemical interaction between the substance to be analysed and the stationary phase. Thus, apart from one chapter dealing with chemically modified silicas, the main theme of the book is developed in three chapters on sample preparation and three on detection.

✦ Table of Contents

Content:
Edited by
Page iii

Copyright page
Page iv

List of Contributors
Page xi

Preface
Pages 1-3
K. Zech

Chapter I Preconcentration and Chromatography on Chemically Modified Silicas with Complexation Properties Original Research Article
Pages 5-32
J.L. Veuthey, M.A. Bagnoud, W. Haerdi

Chapter II Sample Handling in Ion Chromatography Original Research Article
Pages 33-81
P.R. Haddad

Chapter III Whole Blood Sample Clean-Up for Chromatographic Analysis Original Research Article
Pages 82-132
U. Christians, K.-Fr. Sewing

Chapter IV Radio-Column Liquid Chromatography Original Research Article
Pages 133-207
A.C. Veltkamp

Chapter V Modern Post-Column Reaction Detection in High-Performance Liquid Chromatography Original Research Article
Pages 208-259
H. Jansen, R.W. Frei

Chapter VI New Luminescence Detection Techniques Original Research Article
Pages 260-334
C. Gooijer, N.H. Velthorst, R.W. Frei

Chapter VII Continuous Separation Techniques in Flow-Injection Analysis Original Research Article
Pages 335-382
M. Valcárcel, M.D. Luque De Castro

Subject Index
Pages 383-389

Journal of Chromatography Library
Pages 391-394