Gas chromatography-negative chemical ionization mass spectrometry (GC-NCIMS) has been applied to the analysis of 0-and S-glucuronides. The glucuronides were derivatized with pentafluorobenzyl (PFB) bromide and Tri-Sil, and analyzed by GC-NCIMS. All glucuronides gave a large [M-PFBI-ion indicative of
β¦ LIBER β¦
Selective detection of brominated aromatic compounds using gas chromatography/negative chemical ionization mass spectrometry
β Scribed by Buser, Hans Rudolf.
- Book ID
- 126966223
- Publisher
- American Chemical Society
- Year
- 1986
- Tongue
- English
- Weight
- 906 KB
- Volume
- 58
- Category
- Article
- ISSN
- 0003-2700
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We experienced an autopsy case in which a 53-year-old woman committed suicide by ingesting allegedly a certain agricultural chemical. The blood and stomach contents, after extraction with acetonitrile and chloroform, were subjected to analysis by gas chromatography (GC)/negative ion chemical ionizat