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Selective catalytic hydrogenation of the trans, trans isomer from a mixture of 2,4-hexadienes.

✍ Scribed by Gérard Platbrood; Liliane Wilputte-Steinert

Publisher
Elsevier Science
Year
1974
Tongue
French
Weight
107 KB
Volume
15
Category
Article
ISSN
0040-4039

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✦ Synopsis

SELECTIVE CATALYTIC HYDROGENATION OF THE TRANS, TRANS ISOMER FROM

A MIXTURE OF 2,4-HEXADIENES.

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Racemic trans-1A ( translo-metboxy-1,3,4,%,5,1Ob-hexahydro-2H-[ 11 benzopyrano [ 3,4-b] pyridine, see Scheme 1) was obtained in high chemical yield (up to 89%) and with excellent stereoselectivity (95% truns) by catalytic hydrogenationdehalogenation of 7-chloro-lo-methoxy-3,4,4a,Stetrahydro-2H-[ 1 ]