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Selective 1D 1H → 13C → 13C polarization transfer experiments for small organic molecules

✍ Scribed by Leszek Poppe; Stefan Gröger; Jeff Zablocki

Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
56 KB
Volume
37
Category
Article
ISSN
0749-1581

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✦ Synopsis

Selective polarization transfer from proton to adjacent carbon was accomplished by either selective crosspolarization or selective refocused-INEPT. Magnetization was transferred in the subsequent step to remote carbons separated by one, two or three bonds. The acquired data were processed by a new symmetrization protocol resulting in the signal-to-noise ratio enhancement by a factor of p 2.

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